HRID2269449

反应详情

EQUATION

反应方程式

HRID 2269449 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Following a similar procedure to that described in Example (1b), 820 mg of isomer B of N-[(R)-1-(3,5-difluorophenyl)ethyl]-N-[(4-methoxyphenyl)-(3-nitrophenyl)methyl]amine [prepared as described in step (a) above], 1.13 g of nickel chloride hexahydrate and 328 mg of sodium borohydride were reacted, to obtain 480 mg of isomer B of the title compound as a yellow oil.

WORKUP

后处理

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