HRID2269462

反应详情

EQUATION

反应方程式

HRID 2269462 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Following a similar procedure to that described in Example (1b), 2.5 g of N-[1-(3,4-difluorophenyl)ethyl]-N-[(4-fluoro-3-nitrophenyl)-(4-methoxyphenyl)methyl]amine [prepared as described in step (a) above], 3.29 g of nickel chloride hexahydrate and 957 mg of sodium borohydride were reacted, to obtain 1.82 g of the title compound as a yellow oil.

WORKUP

后处理

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