HRID2269464

反应详情

EQUATION

反应方程式

HRID 2269464 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Following a reaction and purification procedure similar to those described in Example (59b), 800 mg of N-[1-(3,4-difluorophenyl)ethyl]-N-[(2-fluoro-5-nitrophenyl)-(4-methoxyphenyl)methyl]amine [prepared as described in step (a) above], 1.05 g of nickel chloride hexahydrate and 306 mg of sodium borohydride were reacted, to obtain 330 mg of isomer A and 350 mg of isomer B of the title compound as yellow oils, respectively.

WORKUP

后处理

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