HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 18334235, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 18347134 | HCID 18347134 | — |
| Catalyst | Dichloronickel;hexahydrate | HCID 11791229 | — |
| Product | HCID 18334235 | HCID 18334235 | 86.1% |
Reaction Steps
Following a similar procedure to that described in Example (1b), 2.80 g of N-[1-(2,4-difluorophenyl)ethyl]-N-[(4-methoxyphenyl)-(3-nitrophenyl)methyl]amine [prepared as described in step (a) above], 3.34 g of nickel chloride hexahydrate and 1.12 g of sodium borohydride were reacted, to obtain 2.23 g of the title compound as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06329405B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-734ebd98f70f48b598e85d838e61e749 |
| Source note | uspto-grants-2001_12 |