Sodium borohydride → HCID 18347089, compound

Participants

Reaction Steps

Following a similar reaction, separation and purification procedure to that described in Example (59b), 2.70 g of N-[1-(3,5-dimethoxyphenyl)ethyl]-N-[(4-fluorophenyl)-(3-nitrophenyl)methyl]amine [prepared as described in step (a) above], 3.13 g of nickel chloride hexahydrate and 1.00 g of sodium borohydride were reacted, to obtain 892 mg of isomer A and 546 mg of isomer B of the title compound as pale yellow oils, respectively.

Provenance & Evidence