Sodium borohydride → HCID 18334248, compound

Participants

Reaction Steps

Following, a similar reaction, separation and purification procedure to that described in Example (59b), 3.39 g of N-[1-(3,5-dichlorophenyl)ethyl]-N-[(4-fluorophenyl)-(3-nitrophenyl)methyl]amine [prepared as described in step (a) above], 3.86 g of nickel chloride hexahydrate and 1.23 g of sodium borohydride were reacted, to obtain 970 mg of isomer A and 567 mg of isomer B of the title compound as a pale yellow oil and a white solid, respectively.

Provenance & Evidence