Sodium borohydride → HCID 18347071, compound

Participants

Reaction Steps

Following a similar reaction, separation and purification procedure to that described in Example (59b), 3.42 g of N-[1-(3,4-difluorophenyl)ethyl]-N-[(4-fluorophenyl)-(3,4-dimethoxy-5-nitrophenyl)methyl]amine [prepared as described in step (a) above], 3.65 g of nickel chloride hexahydrate and 1.17 g of sodium borohydride were reacted, to obtain 1.10 g of isomer A and 1.39 g of isomer B of the title compound as pale yellow oils, respectively.

Provenance & Evidence