HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 18334152, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 18334205 | HCID 18334205 | — |
| Catalyst | Dichloronickel;hexahydrate | HCID 11791229 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18334152 | HCID 18334152 | — |
Reaction Steps
Following a similar procedure to that described in Example (1b), 720 mg of isorner B of N-[1-(3,4-difluorophenyl)ethyl]-N-[(2,4-dimethoxyphenyl)-(3-nitrophenyl)methyl]amine [prepared as described in step (a) above], 799 mg of nickel chloride hexahydrate, 254 mg of sodium borohydride and 80 ml of methanol were reacted, to obtain 580 mg of isomer B of the title compound as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06329405B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-fb3e60a45a0840af9a099701de17c868 |
| Source note | uspto-grants-2001_12 |