HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 70189115, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 18334081 | HCID 18334081 | — |
| Catalyst | Dichloronickel;hexahydrate | HCID 11791229 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 70189115 | HCID 70189115 | 94.6% |
Reaction Steps
Following a similar procedure to that described in Example (94b), 1.39 g of N-[(4-methoxyphenyl)-(3-nitrophenyl)methyl]-N-(1-methyl-1-phenylethyl)amine [prepared as described in step (a) above], 1.76 g of nickel chloride hexahydrate, 559 mg of sodium borohydride and 100 ml of methanol were reacted, to obtain 1.21 g of the title compound as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06329405B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-758f9eb6510b4fc5866ea9103a1ee204 |
| Source note | uspto-grants-2001_12 |