HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Cyclobutene-1,2-dione, 3-(1,1-dimethylethoxy)-4-methoxy- → HCID 86757668, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Cyclobutene-1,2-dione, 3-(1,1-dimethylethoxy)-4-methoxy- | HCID 10559380 | — |
| Reactant | HCID 70189115 | HCID 70189115 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86757668 | HCID 86757668 | 82.9% |
Reaction Steps
Following a similar procedure to that described in Example (94c), 1.19 g of 3-[(4-methoxyphenyl)-(1-methyl-1-phenylethylamino)methyl]phenylamine [prepared as described in step (b) above], 886 mg of 3-t-butoxy-4-methoxy-3-cyclobutene-1,2-dione and 40 ml of methanol were reacted, to obtain 1.42 g of the title compound as a white foamy solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06329405B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-3de26452f0584ba89cdbc833e3416eae |
| Source note | uspto-grants-2001_12 |