HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 86757667, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 86757668 | HCID 86757668 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86757667 | HCID 86757667 | 99.8% |
Reaction Steps
Following a similar procedure to that described in Example (55b), 1.40 g of 3-t-butoxy-4-{3-[(4-methoxyphenyl )-(1-methyl-1-phenylethylamino)methyl]phenylamino}-3-cyclobutene-1,2-dione [prepared as described in step (c) above], 10 ml of trifluoroacetic acid and 35 ml of dichloromethane were reacted, to obtain 1.24 g of the title compound as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06329405B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-7fc7f7429e4945f59d89e19d1aa60686 |
| Source note | uspto-grants-2001_12 |