Sodium borohydride → HCID 18347023, compound

Participants

Reaction Steps

Following a similar reaction, separation and purification procedure to that described in Example (59b), 3.96 g of N-[(4-chlorophenyl)-(3-nitrophenyl)methyl]-N-[1-(2,3,4-trifluorophenyl)ethyl]amine [prepared as described in step (a) above], 4.47 g of nickel chloride hexahydrate and 1.42g of sodium borohydride were reacted, to obtain 1.05 g of isomer A and 720 mg, of isomer B of the title compound, each as a pale yellow oil.

Provenance & Evidence