HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 70190185, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 70188095 | HCID 70188095 | — |
| Catalyst | Dichloronickel;hexahydrate | HCID 11791229 | — |
| Product | HCID 70190185 | HCID 70190185 | 96.2% |
Reaction Steps
Following a similar procedure to that described in Example (1b), 2.61 g of N-[(4-methoxyphenyl)-(3-nitrophenyl)methyl]-N-[(R)-1-(3,4,5-trifluorophenyl)ethyl]amine [prepared as described in step (a) above], 3.00 g of nickel chloride hexahydrate and 958 mg of sodium borohydride were reacted, to obtain 2.33 g of the title compound as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06329405B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-df4a2775aca44c31a1df5dbc881a993d |
| Source note | uspto-grants-2001_12 |