Sodium borohydride → HCID 18334079, compound

Participants

Reaction Steps

Following a similar reaction, separation and purification procedure to that described in Example (1b). 2.07 g of N-[1-(3,4-difluorophenyl)ethyl]-N-[(3-nitrophenyl)(pyridin-4-yl)methyl]amine [prepared as described in step (a) above], 2.66 g of nickel chloride hexahydrate and 848 mg of sodium borohydride were reacted, to obtain 684 mg of the title compound as a colorless oil.

Provenance & Evidence