Sodium borohydride → HCID 70188091, compound

Participants

Reaction Steps

Following a procedure similar to that described in Example (59b), 2.06 g of N-[(4-methoxyphenyl)-(3-nitrophenyl)methyl]-N-[(R)-1-phenylethyl]amine [prepared as described in step (a) above], 2.70 g of nickel chloride hexahydrate and 860 mg of sodium borohydride were reacted, separated and purified, to obtain 510 mg of isomer A and 672 mg of isomer B of the title compound, each as a yellow oil.

Provenance & Evidence