HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 70189766, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 70189330 | HCID 70189330 | — |
| Catalyst | Dichloronickel;hexahydrate | HCID 11791229 | — |
| Product | HCID 70189766 | HCID 70189766 | 93.9% |
Reaction Steps
Following a procedure similar to that described in Example (1b), 1.56 g of N-[phenyl-(3-nitrophenyl)methyl]-N-[(R)-1-(napthalen-1-yl)ethyl]amine [prepared as described in step (a) above], 2.23 g of nickel chloride hexahydrate and 650 mg of sodium borohydride were reacted, to obtain 1.35 g of the title compound as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06329405B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-b1c9432a2b3d497ba3e1301d12a2a9a2 |
| Source note | uspto-grants-2001_12 |