HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 70188141, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 70189245 | HCID 70189245 | — |
| Catalyst | Dichloronickel;hexahydrate | HCID 11791229 | — |
| Product | HCID 70188141 | HCID 70188141 | 100.3% |
Reaction Steps
Following a procedure similar to that described in Example (1B), 1.51 g of N-[p-tolyl-(3-nitrophenyl)methyl]-N-[(R)-1-(naphthalen-1-yl)ethyl]amine [prepared as described in step (a) above], 2.08 g of nickel chloride hexahydrate and 607 mg of sodium borohydride were reacted, separated and purified, to obtain 1.40 g of the title compound as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06329405B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-64c3ee231cb3403e8e84de3a4d087155 |
| Source note | uspto-grants-2001_12 |