HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromohexadecane → HCID 46178576, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromohexadecane | HCID 8213 | — |
| Reactant | 1-Vinylimidazole | HCID 66171 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 46178576 | HCID 46178576 | — |
Reaction Steps
15 g of N-vinylimidazole and 50 g of 1-bromohexadecane were stirred in a 500 ml vessel at 60° C. for 8 h. Then, 100 ml of ethyl acetate were added to this mixture while stirring. After a clear solution had formed, the heating and stirring was switched off. A colorless crystalline precipitate formed during the cooling to room temperature and was filtered off and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06329483B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-f5c1959491384a30885a0168abea818b |
| Source note | uspto-grants-2001_12 |