1-Bromohexadecane → HCID 46178576, compound

HRID 2269585Notes

Reaction equation

HRID 2269585 reaction equation
[CH:1]([N:3]1[CH:7]=[CH:6][N:5]=[CH:4]1)=[CH2:2].[Br:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24]>C(OCC)(=O)C>[Br-:8].[CH2:9]([N+:5]1[CH:6]=[CH:7][N:3]([CH:1]=[CH2:2])[CH:4]=1)[CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24]

Participants

4

Reactant 2

HCID 82131-BromohexadecaneHCID 661711-Vinylimidazole

Product 1

HCID 46178576HCID 46178576, compound

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent

Procedure

15 g of N-vinylimidazole and 50 g of 1-bromohexadecane were stirred in a 500 ml vessel at 60° C. for 8 h. Then, 100 ml of ethyl acetate were added to this mixture while stirring. After a clear solution had formed, the heating and stirring was switched off. A colorless crystalline precipitate formed during the cooling to room temperature and was filtered off and dried.

Workup

  1. customAfter a clear solution had formed
  2. stirringthe heating and stirring
  3. customA colorless crystalline precipitate formed during the cooling to room temperature
  4. filtrationwas filtered off
  5. customdried

Sources & evidence

ORD record
ord-f5c1959491384a30885a0168abea818b
Source dataset
uspto-grants-2001_12
Patent number
US06329483B1

Reaction notes

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