HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178500755, compound → 3-(3,4-dimethyl-benzoyl)-7-fluoro-1H-quinolin-4-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178500755 | HCID 178500755 | — |
| Solvent | Diphenyl Ether | HCID 7583 | — |
| Product | 3-(3,4-dimethyl-benzoyl)-7-fluoro-1H-quinolin-4-one | HCID 57754794 | 79.8% |
Reaction Steps
Compound 3k was prepared following the procedure described in Step 2 of Example 5 using 1.19 g (3.64 mmol) of 2-(3,4-Dimethyl-benzoyl)-3-(3-fluoro-phenylamino)-acrylic acid methyl ester 2h and 30 mL of diphenyl ether to yield 0.858 g of 3-(3,4-dimethyl-benzoyl)-7-fluoro-1H-quinolin-4-one 3k as a brown solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07557213B2 |
| Source dataset | uspto-grants-2009_07 |
| ORD ID | ord-cc24c7b698c24ce3a98d2134a5e54928 |
| Source note | uspto-grants-2009_07 |