HRID2269675

反应详情

EQUATION

反应方程式

HRID 2269675 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a 300 ml four necked flask, 13.56 g (0.10 mol) of 2-fluoro-1,3-dimethylimidazolidine (DFI), 15.0 g (0.10 mol) of sodium iodide and 125 g of acetonitrile were charged and reacted at 25° C. for 4 hours in a nitrogen atmosphere under light shielding. The yield of 2-fluoro-1,3-dimethylimidazolinium=iodide (DMFI) was 95%.

WORKUP

后处理

  1. customreacted at 25° C. for 4 hours in a nitrogen atmosphere under light shielding