HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18188678, compound → HCID 18188573, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18188678 | HCID 18188678 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18188573 | HCID 18188573 | — |
Reaction Steps
A mixture of Example 27E (0.5 g, 1.04 mmol) and 10% palladium on carbon (50 mg) in methanol (50 mL) was shaken under hydrogen gas (balloon) for 6 hours, filtered through diatomaceous earth (Celite®), and concentrated to provide the desired product. MS (ESI(−)Q1MS) m/z 278 (M−H)−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06329534B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-a77f8ef0b9d04005a8799dccc7ce5036 |
| Source note | uspto-grants-2001_12 |