HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 22632938, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Reactant | Benzyloxyamine hydrochloride | HCID 102312 | — |
| Reactant | HCID 22632869 | HCID 22632869 | — |
| Product | HCID 22632938 | HCID 22632938 | 102% |
Reaction Steps
Using General Method 2, the reaction of carbonyldiimidazole (3.6 g, 22.4 mmol), 2-(4methoxy-anilino)-4,5-difluorobenzoic acid (Example O, 5.72 g, 20.4 mmol), O-benzylhydroxylamine hydrochloride (3.26 g, 20.4 mmol), and triethylamine (3.1 mL, 22.4 mmol) provided 8.0 g of the crude title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06331538B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-d68e684ff5b7495b86dd57ee38f9d2b6 |
| Source note | uspto-grants-2001_12 |