HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22633026, compound → HCID 22632949, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22633026 | HCID 22633026 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 22632949 | HCID 22632949 | 88.5% |
Reaction Steps
Using the General Method 6A, the reaction of 10% Pd/C (0.03 g) with 1-(2-fluorophenyl)-6-fluoro-3-benzyloxy-7-pyrrolidin-1-yl-1H-quinazoline-2,4-dione (Example W-1, 0g, 0.22 mmol) provided 0.07 g of the title compound as a solid, mp 235-237° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06331538B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-f53a402c298e443286fead5aa8ac5d29 |
| Source note | uspto-grants-2001_12 |