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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2270302Generated: October 31, 2026

HCID 22633008, compound → HCID 22632934, compound

https://huagongshe.com/reaction/2270302

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 22633008HCID 22633008—
CatalystPalladiumHCID 23938—
SolventTetrahydrofuranHCID 8028—
ProductHCID 22632934HCID 22632934116.4%

Reaction Steps

Using the method of Example 56, 20% Pd/C (25 mg), 3-benzyloxy-1-(2-fluorophenyl)-6-fluoro-7-pyrrolidin-1-yl-1H-pyrido[2,3-d]pyrimidine-2,4dione (Example T-4, 0.14 g, 0.31 mmol) were combined in 25 mL of THF, to give 0.13 g of the title compound as a solid, mp >250° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06331538B1
Source datasetuspto-grants-2001_12
ORD IDord-122a32d6f4ce4dc2a9e3f31d87a459f5
Source noteuspto-grants-2001_12