Diethanolamine → HCID 784350, compound

HRID 2270369Notes

Reaction equation

HRID 2270369 reaction equation
[NH:1]([CH2:5][CH2:6][OH:7])[CH2:2][CH2:3][OH:4].[Br:8][C:9]1[CH:16]=[CH:15][C:12]([CH2:13]Br)=[CH:11][CH:10]=1>>[Br:8][C:9]1[CH:16]=[CH:15][C:12]([CH2:13][N:1]([CH2:5][CH2:6][OH:7])[CH2:2][CH2:3][OH:4])=[CH:11][CH:10]=1

Participants

3

Reactant 2

HCID 8113DiethanolamineHCID 685274-Bromobenzyl bromide

Product 1

HCID 784350HCID 784350, compound

Procedure

2-[(4-Bromobenzyl)-(2-hydroxy-ethyl)-amino]-ethanol was prepared according to the general method as outlined in example 83. Starting from diethanolamine (22.5 g,, 150 mmol). and 4-bromobenzyl bromide (25 g, 100 mmol). Yield 33.66 g, (99%); yellow oil; MS: 273.8 (M+H)+.

Sources & evidence

ORD record
ord-4569d36129ed428a953e21806181046d
Source dataset
uspto-grants-2001_12
Patent number
US06331563B1

Reaction notes

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