Diethanolamine → Ethanol, 2,2'-[(3-phenylpropyl)imino]bis-

HRID 2270371Notes

Reaction equation

HRID 2270371 reaction equation
[NH:1]([CH2:5][CH2:6][OH:7])[CH2:2][CH2:3][OH:4].Br[CH2:9][CH2:10][CH2:11][C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1>>[OH:4][CH2:3][CH2:2][N:1]([CH2:9][CH2:10][CH2:11][C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1)[CH2:5][CH2:6][OH:7]

Participants

3

Reactant 2

HCID 8113DiethanolamineHCID 12503(3-Bromopropyl)benzene

Product 1

HCID 11770082Ethanol, 2,2'-[(3-phenylpropyl)imino]bis-

Procedure

2-[(2-Hydroxy-ethyl)-(3-phenyl-propyl)-amino]-ethanol was prepared according to the general method as outlined in example 83. Starting from diethanolamine (15.8 g, 151 mmol). and 1-bromo-3-phenylpropane (20 g, 101 mmol). Yield 21.31 g, (95%); yellow oil; MS: 223.9 (M+H)+.

Sources & evidence

ORD record
ord-645f19dae0fa4f359874d6e927a49a08
Source dataset
uspto-grants-2001_12
Patent number
US06331563B1

Reaction notes

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