HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethanolamine → Ethanol, 2,2'-[(3-phenoxypropyl)imino]bis-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethanolamine | HCID 8113 | — |
| Reactant | Benzene, (3-bromopropoxy)- | HCID 68522 | — |
| Product | Ethanol, 2,2'-[(3-phenoxypropyl)imino]bis- | HCID 10922638 | — |
Reaction Steps
2-[(2-Hydroxy-ethyl)-(3-phenoxy-propyl)-amino]-ethanol was prepared according to the general method as outlined in example 83. Starting from diethanolamine (15.8 g, 151 mmol). and 3-Phenoxypropyl bromide (21.5 g, 100 mmol). Yield 21.31 g, (95%); yellow oil; MS: 238.1 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06331563B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-6aa4ae5bec484cc0804eff830e0b6a08 |
| Source note | uspto-grants-2001_12 |