Diethanolamine → Ethanol, 2,2'-[(3-phenoxypropyl)imino]bis-

HRID 2270388Notes

Reaction equation

HRID 2270388 reaction equation
[NH:1]([CH2:5][CH2:6][OH:7])[CH2:2][CH2:3][OH:4].[O:8]([CH2:15][CH2:16][CH2:17]Br)[C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1>>[OH:4][CH2:3][CH2:2][N:1]([CH2:17][CH2:16][CH2:15][O:8][C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1)[CH2:5][CH2:6][OH:7]

Participants

3

Reactant 2

HCID 8113DiethanolamineHCID 68522Benzene, (3-bromopropoxy)-

Product 1

HCID 10922638Ethanol, 2,2'-[(3-phenoxypropyl)imino]bis-

Procedure

2-[(2-Hydroxy-ethyl)-(3-phenoxy-propyl)-amino]-ethanol was prepared according to the general method as outlined in example 83. Starting from diethanolamine (15.8 g, 151 mmol). and 3-Phenoxypropyl bromide (21.5 g, 100 mmol). Yield 21.31 g, (95%); yellow oil; MS: 238.1 (M+H)+.

Sources & evidence

ORD record
ord-6aa4ae5bec484cc0804eff830e0b6a08
Source dataset
uspto-grants-2001_12
Patent number
US06331563B1

Reaction notes

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