Diethanolamine → HCID 11770129, compound

HRID 2270392Notes

Reaction equation

HRID 2270392 reaction equation
[NH:1]([CH2:5][CH2:6][OH:7])[CH2:2][CH2:3][OH:4].Cl[C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=1[O:15][CH2:16][CH3:17]>>[OH:4][CH2:3][CH2:2][N:1]([CH2:17][CH2:16][O:15][C:10]1[CH:11]=[CH:12][CH:13]=[CH:14][CH:9]=1)[CH2:5][CH2:6][OH:7]

Participants

3

Reactant 2

HCID 8113DiethanolamineHCID 691971-Chloro-2-ethoxybenzene

Product 1

HCID 11770129HCID 11770129, compound

Procedure

2-[(2-Hydroxy-ethyl)-(2-phenoxy-ethyl)-amino]-ethanol was prepared according to the general method as outlined in example 83. Starting from diethanolamine (15.0 g, 150). and 2chloro-phenetol (15.6 g, 100 mmol). Yield 18 g, (80%); Colorless oil; MS: 226 (M+H)+.

Sources & evidence

ORD record
ord-f188c19104fb466db28a99f499031aa6
Source dataset
uspto-grants-2001_12
Patent number
US06331563B1

Reaction notes

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