Iodoethane → HCID 18331409, compound

HRID 2270545Notes

Reaction equation

[NH2:1][C:2]1[C:3]([NH:8][C:9]2[CH:14]=[CH:13][CH:12]=[C:11]([CH2:15][N:16]([C:24]([O:26][C:27]([CH3:30])([CH3:29])[CH3:28])=[O:25])[C:17]([O:19][C:20]([CH3:23])([CH3:22])[CH3:21])=[O:18])[CH:10]=2)=[N:4][CH:5]=[CH:6][CH:7]=1.[CH2:31](I)[CH3:32]>>[CH2:31]([NH:1][C:2]1[C:3]([NH:8][C:9]2[CH:14]=[CH:13][CH:12]=[C:11]([CH2:15][N:16]([C:24]([O:26][C:27]([CH3:30])([CH3:29])[CH3:28])=[O:25])[C:17]([O:19][C:20]([CH3:23])([CH3:22])[CH3:21])=[O:18])[CH:10]=2)=[N:4][CH:5]=[CH:6][CH:7]=1)[CH3:32]

Participants

Reactant 2

HCID 6340Iodoethane

HCID 18331432HCID 18331432, compound

Product 1

HCID 18331409HCID 18331409, compoundYield 54%

Procedure

Using the compound obtained in Example 3 as a starting material and also using ethyl iodide as a reagent, the procedure of Example 5 was repeated to give the titled compound (yield, 54%).

Sources & evidence

ORD record: ord-ca275645d89545989539e50786f7510c
Source dataset: uspto-grants-2001_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06331553B1

Reaction notes

Loading…