Oxalyl chloride → HCID 22742433, compound

HRID 2270915Notes

Reaction equation

HRID 2270915 reaction equation
[CH3:1][C:2]1[CH:3]=[CH:4][C:5]2[C:6](=O)[C:7]3[C:12]([N:13]([CH2:17][CH2:18][CH2:19][N:20]4[C:24](=[O:25])[C:23]5=[CH:26][CH:27]=[CH:28][CH:29]=[C:22]5[C:21]4=[O:30])[C:14]=2[C:15]=1[CH3:16])=[CH:11][CH:10]=[CH:9][CH:8]=3.C(Cl)(=O)C([Cl:35])=O>ClCCl>[Cl-:35].[CH3:1][C:2]1[CH:3]=[CH:4][C:5]2[C:14]([C:15]=1[CH3:16])=[N+:13]([CH2:17][CH2:18][CH2:19][N:20]1[C:24](=[O:25])[C:23]3=[CH:26][CH:27]=[CH:28][CH:29]=[C:22]3[C:21]1=[O:30])[C:12]1[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=1)[C:6]=2[Cl:35]

Participants

4

Reactant 2

HCID 65578Oxalyl chlorideHCID 227424473,4-Dimethyl-10-(3-phthalimidopropyl)-9-acridone

Product 1

HCID 22742433HCID 22742433, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

A mixture of 1.0 g of 3,4-dimethyl-10-(3-phthalimidopropyl)-9-acridone with 340 ml of oxalyl chloride was stirred at room temperature in 100 ml of dichloromethane for 30 min. After evaporating the excessive oxalyl chloride and dichloromethane under reduced pressure, 1.1 g of the title compound was obtained.

Workup

  1. customAfter evaporating the excessive oxalyl chloride and dichloromethane under reduced pressure

Sources & evidence

ORD record
ord-7def27292f2542b08ca4ab0b1e4e0361
Source dataset
uspto-grants-2001_12
Patent number
US06333322B1

Reaction notes

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