Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Thiourea | HCID 2723790 | — |
| Reactant | HCID 18330803 | HCID 18330803 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 18330802 | HCID 18330802 | — |
Reaction Steps
0.5 g of 2-[4-(dimethylamino)phenyl]-2-oxo-1-phenylethyl benzoate is dissolved in 10 ml of dimethylformamide in a reactor. 0.212 g of thiourea (2 eq.) is subsequently added and the reaction mixture is left to react at reflux (160° C.) for 6 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06333414B1 |
|---|
| Source dataset | uspto-grants-2001_12 |
|---|
| ORD ID | ord-2e53d88ea1514e22888599550d2e00b5 |
|---|
| Source note | uspto-grants-2001_12 |
|---|
