Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Thiourea | HCID 2723790 | — |
| Reactant | HCID 70216051 | HCID 70216051 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 18330796 | HCID 18330796 | — |
Reaction Steps
0.15 g of 3,3-dimethyl-2-oxo-1-phenylbutyl benzoate is dissolved in 8 ml of dimethylformamide in a reactor. 0.2 g of thiourea (5 eq.) is subsequently added and the reaction mixture is left to react at reflux (160° C.) for 15 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06333414B1 |
|---|
| Source dataset | uspto-grants-2001_12 |
|---|
| ORD ID | ord-74e74c17e3e14f12aa087305aca1ab60 |
|---|
| Source note | uspto-grants-2001_12 |
|---|
