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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2271497Generated: November 1, 2026

Hydrochloric Acid → HCID 70676330, compound

https://huagongshe.com/reaction/2271497

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 70676150HCID 70676150—
SolventMethanolHCID 887—
ProductHCID 70676330HCID 7067633097%

Reaction Conditions

Temperature60 °C

Reaction Steps

1N HCl (3 mL) was added to 10 mL of tertiary butyl 3-((3,4-dichlorophenyl)(phenoxy)methyl)azetidine-1-carboxylate (150 mg, 0.352 mmol) dissolved in a methanol solution, and heated to reflux at 60° C. for one day. Thereafter, the solvent of the reaction mixture was removed by reduced pressure evaporation to obtain the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09120771B2
Source datasetuspto-grants-2015_09
ORD IDord-93bc20a08d9041a0b7ad8d0f4530eab1
Source noteuspto-grants-2015_09