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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2271501Generated: November 1, 2026

Hydrochloric Acid → HCID 86722613, compound

https://huagongshe.com/reaction/2271501

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantMethanolHCID 887—
ReactantHCID 86722612HCID 86722612—
ProductHCID 86722613HCID 8672261397%

Reaction Conditions

Temperature60 °C

Reaction Steps

1 N HCl (3.0 mL) was added to 10 mL of tertiary butyl 3-(1-(3,4-dichlorophenyl)-2-(methylsulfonyl)ethyl)azetidine-1-carboxylate (0.15 g, 0.36 mmol) dissolved in the methanol solution and heated to reflux at 60° C. for one day. Thereafter, the solvent of the reaction mixture was removed by reduced pressure evaporation to obtain the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09120771B2
Source datasetuspto-grants-2015_09
ORD IDord-b84ee1e4de4942dd8cd64db1e509e761
Source noteuspto-grants-2015_09