HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Boc-4-(aminomethyl)piperidine → HCID 68091878, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Boc-4-(aminomethyl)piperidine | HCID 736817 | — |
| Reactant | (6-Bromo-4-chloroquinolin-3-yl)(cyclopropyl)methanone | HCID 66715111 | — |
| Product | HCID 68091878 | HCID 68091878 | 99% |
Reaction Steps
Following general procedure B, (6-bromo-4-chloroquinolin-3-yl)(cyclopropyl)methanone (500 mg, 1.60 mmol) was reacted with tert-butyl 4-(aminomethyl)piperidine-1-carboxylate (516 mg, 2.41 mmol) to afford the desired product (80 mg, >99%) as an orange foam: ESI MS m/z 489 [C24H30BrN3O3+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09120749B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-06f4b551cce1440784168ccfc6d7570c |
| Source note | uspto-grants-2015_09 |