HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(6-Bromo-4-chloroquinolin-3-YL)ethanone → HCID 178467071, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(6-Bromo-4-chloroquinolin-3-YL)ethanone | HCID 66715483 | — |
| Reactant | HCID 178419079 | HCID 178419079 | — |
| Product | HCID 178467071 | HCID 178467071 | 80.4% |
Reaction Steps
Following general procedure B, 1-(6-bromo-4-chloroquinolin-3-yl)ethanone (420 mg, 1.48 mmol) was reacted with tert-butyl trans-4-aminocyclohexylcarbamate (642 mg, 3.00 mmol) to afford the desired product (550 mg, 80%) as an off-white solid: ESI MS m/z 462 [C22H28BrN3O3+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09120749B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-b18b5a583ca74c2ab6efd6d083a6d454 |
| Source note | uspto-grants-2015_09 |