HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Dimethylaminomethyl)piperidine → HCID 66715563, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Dimethylaminomethyl)piperidine | HCID 11137268 | — |
| Reactant | 1-(6-Bromo-4-chloroquinolin-3-YL)ethanone | HCID 66715483 | — |
| Product | HCID 66715563 | HCID 66715563 | 8.1% |
Reaction Steps
Following general procedure B, 1-(6-bromo-4-chloroquinolin-3-yl)ethanone (160 mg, 0.560 mmol) was reacted with N,N-dimethyl-1-(piperidin-4-yl)methanamine (172 mg, 0.800 mmol) to afford the desired product (17.7 mg, 8%) as an off-white solid: ESI MS m/z 390 [C19H24BrN3O+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09120749B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-45b271ef61bd44e487c2d9226956cea7 |
| Source note | uspto-grants-2015_09 |