HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-butyl N-(4-oxocyclohexyl)carbamate → HCID 86692878, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-butyl N-(4-oxocyclohexyl)carbamate | HCID 1512535 | — |
| Reactant | (3R)-3-fluoropyrrolidine hydrochloride | HCID 2759162 | — |
| Product | HCID 86692878 | HCID 86692878 | 51% |
Reaction Steps
Following General procedure I, (R)-3-fluoropyrrolidine hydrochloride (407 mg, 3.26 mmol) was reacted with tert-butyl 4-oxocyclohexylcarbamate (500 mg, 2.34 mmol) to afford the desired product (200 mg, 51%) as a colorless oil: ESI MS m/z 187 [C10H19FN2+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09120749B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-127d6a7df3544c36aea14457af7b3c17 |
| Source note | uspto-grants-2015_09 |