HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-butyl N-(4-oxocyclohexyl)carbamate → HCID 66715482, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-butyl N-(4-oxocyclohexyl)carbamate | HCID 1512535 | — |
| Reactant | 3,3-Difluoropyrrolidine hydrochloride | HCID 24903482 | — |
| Product | HCID 66715482 | HCID 66715482 | 106.1% |
Reaction Steps
Following General procedure I, 3,3-difluoropyrrolidine hydrochloride (468 mg, 3.26 mmol) was reacted with tert-butyl 4-oxocyclohexylcarbamate (500 mg, 2.34 mmol) to afford the desired product (507 mg, quant.) as a colorless oil: ESI MS m/z 205 [C10H18F2N2+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09120749B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-ab46db9db883481981fef8c8dcd2acdd |
| Source note | uspto-grants-2015_09 |