Ammonium Chloride → HCID 86609040, compound

HRID 227248Notes

Reaction equation

HRID 227248 reaction equation
CO[C:3]1[CH2:4][N:5]([C:10]([O:12][C:13]([CH3:16])([CH3:15])[CH3:14])=[O:11])[CH2:6][CH2:7][CH2:8][N:9]=1.[Cl-:17].[NH4+:18]>C(O)C>[ClH:17].[NH:18]=[C:3]1[N:9]=[CH:8][CH:7]=[CH:6][N:5]([C:10]([O:12][C:13]([CH3:16])([CH3:15])[CH3:14])=[O:11])[CH2:4]1

Participants

4

Reactant 2

HCID 25517Ammonium ChlorideHCID 541055031,1-Dimethylethyl 2,5,6,7-tetrahydro-3-methoxy-1H-1,4-diazepine-1-carboxylate

Product 1

HCID 86609040HCID 86609040, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

To a stirred solution of imino methyl ether from Step A (1.75 g, 7.66 mmol) in ethanol was added ammonium chloride (0.4 g, 7.68 mmol). The resultant mixture was refluxed for 4 h. Concentration gave the title compound.

Workup

  1. concentrationConcentration

Sources & evidence

ORD record
ord-717e459986cd455c92cde8e470020a9f
Source dataset
uspto-grants-2009_07
Patent number
US07560455B2

Reaction notes

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