HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Chloride → HCID 86609040, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Chloride | HCID 25517 | — |
| Reactant | 1,1-Dimethylethyl 2,5,6,7-tetrahydro-3-methoxy-1H-1,4-diazepine-1-carboxylate | HCID 54105503 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86609040 | HCID 86609040 | — |
Reaction Steps
To a stirred solution of imino methyl ether from Step A (1.75 g, 7.66 mmol) in ethanol was added ammonium chloride (0.4 g, 7.68 mmol). The resultant mixture was refluxed for 4 h. Concentration gave the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07560455B2 |
| Source dataset | uspto-grants-2009_07 |
| ORD ID | ord-717e459986cd455c92cde8e470020a9f |
| Source note | uspto-grants-2009_07 |