4-Cyanobenzoic acid → HCID 86729764, compound

HRID 2272607Notes

Reaction equation

HRID 2272607 reaction equation
[NH2:1][CH2:2][CH:3]([CH3:23])[C:4]([NH:6][CH2:7][C:8]1[CH:9]=[CH:10][C:11]2[N:12]([CH2:21][CH3:22])[C:13]3[C:18]([C:19]=2[CH:20]=1)=[CH:17][CH:16]=[CH:15][CH:14]=3)=[O:5].[C:24]([C:26]1[CH:34]=[CH:33][C:29]([C:30](O)=[O:31])=[CH:28][CH:27]=1)#[N:25]>>[C:24]([C:26]1[CH:34]=[CH:33][C:29]([C:30]([NH:1][CH2:2][CH:3]([CH3:23])[C:4]([NH:6][CH2:7][C:8]2[CH:9]=[CH:10][C:11]3[N:12]([CH2:21][CH3:22])[C:13]4[C:18]([C:19]=3[CH:20]=2)=[CH:17][CH:16]=[CH:15][CH:14]=4)=[O:5])=[O:31])=[CH:28][CH:27]=1)#[N:25]

Participants

3

Reactant 2

HCID 120874-Cyanobenzoic acidHCID 86729765HCID 86729765, compound

Product 1

HCID 86729764HCID 86729764, compound

Procedure

Using the compound obtained in Step 2 and 4-cyanobenzoic acid, and by the reaction and purification in the same manner as in the method described in Step 3 of Example 36, the title compound was obtained.

Workup

  1. customby the reaction and purification in the same manner as in the method

Sources & evidence

ORD record
ord-30ef2a9a69dc402facfe103ac8413e5d
Source dataset
uspto-grants-2015_09
Patent number
US09120776B2

Reaction notes

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