Ethanol → HCID 87486712, compound

Participants

Reaction Steps

0.60 g (3.5 mmole) anhydrous tosylic acid was dissolved in possibly as little as ethanol. Then a solution of 0.55 g (0.38 mmole) N-(1-methylethyl)-2,3-dimethyl-2-butylamine in 10 mL anhydrous ether was added dropwise with stirring. The mixture was stood overnight, and then distilled off the solvent. The residue was washed thoroughly with anhydrous ethanol to give a colorless solid 1.07 g, mp 119-120° C. 1H-NMR(D2O, ppm) 0.96(d, 6H, 2CH3), 1.303(s, 6H, 2CH3), 1.36(d, 6H, 2CH3), 2.02-2.15(m, 1H, C(H), 2.401(s, 3H, CH3), 3.62-3.73(m, 1H, CH), 7.38(d,2H, 2Ar—H), 7.70(d,2H, 2Ar—H).

Provenance & Evidence