HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 71765124, compound → HCID 71765123, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 71765124 | HCID 71765124 | — |
| Reactant | HCID 89826303 | HCID 89826303 | — |
| Product | HCID 71765123 | HCID 71765123 | — |
Reaction Steps
7-fluoro-3-[4-(4-hydroxy-1-methylene-butyl)-phenyl]-2H-pyrrolo[1,2-a]pyrazin-1-one (contains some of the isomer 7-fluoro-3-[4-((E)-4-hydroxy-1-methyl-but-1-enyl)-phenyl]-2H-pyrrolo[1,2-a]pyrazin-1-one); HPLC/MS 2.32 (B), [M+H] 313; 1H NMR (400 MHz, DMSO-d6) δ ppm 10.98 (s, 1H), 7.69-7.53 (m, 3H), 7.53-7.43 (m, 3H), 6.75 (m, 1H), 6.45-6.39 (m, 2H), 4.41 (t, J=5.2 Hz, 1H), 3.45 (td, J=6.4, 5.0 Hz, 2H), 2.29-2.19 (m, 2H), 1.66-1.54 (m, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09120805B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-2dd72a22a0724bfdb1f7211938aca3da |
| Source note | uspto-grants-2015_09 |