HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 178465949, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 86600732 | HCID 86600732 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | HCID 178465949 | HCID 178465949 | — |
Reaction Steps
88 mg (0.25 mmol) 5-acetyl-3-[(methoxycarboxymethyl-amino)-phenyl-methylidene]-2-indolinone (Example 1.005) are suspended in 0.5 ml 1 N sodium hydroxide solution and 5 ml of methanol and refluxed for 4 h. Then the mixture is cooled, 0.5 ml 1 N hydrochloric acid are added and the precipitate is removed by suction filtering.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07560480B2 |
| Source dataset | uspto-grants-2009_07 |
| ORD ID | ord-c01f77f0e9de40b38777b50187d91e0b |
| Source note | uspto-grants-2009_07 |