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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2273526Generated: November 1, 2026

Potassium Carbonate → HCID 57500343, compound

https://huagongshe.com/reaction/2273526

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
ReactantHCID 57500341HCID 57500341—
SolventMethanolHCID 887—
SolventDichloromethaneHCID 6344—
ProductHCID 57500343HCID 5750034383%

Reaction Steps

1.15 g (8.33 mmol) of potassium carbonate are added to the solution of 0.90 g (1.67 mmol) of methyl 5-{[8-(benzyloxy)-1-methoxy-2-methylindolizin-3-yl]carbonyl}-2-[(trifluoroacetyl)amino]benzoate in 100 ml of methanol and 100 ml of dichloromethane. The mixture is stirred at ambient temperature for 20 hours. The yellow precipitate formed is filtered, washed thoroughly with water and dried, to give 0.61 g (83%) of a yellow powder.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09120819B2
Source datasetuspto-grants-2015_09
ORD IDord-09f9fdb112444c9eb2382dbe19c0de1b
Source noteuspto-grants-2015_09