HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 57500343, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 57500341 | HCID 57500341 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 57500343 | HCID 57500343 | 83% |
Reaction Steps
1.15 g (8.33 mmol) of potassium carbonate are added to the solution of 0.90 g (1.67 mmol) of methyl 5-{[8-(benzyloxy)-1-methoxy-2-methylindolizin-3-yl]carbonyl}-2-[(trifluoroacetyl)amino]benzoate in 100 ml of methanol and 100 ml of dichloromethane. The mixture is stirred at ambient temperature for 20 hours. The yellow precipitate formed is filtered, washed thoroughly with water and dried, to give 0.61 g (83%) of a yellow powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09120819B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-09f9fdb112444c9eb2382dbe19c0de1b |
| Source note | uspto-grants-2015_09 |