Diethyl Ether → HCID 57500384, compound

Participants

Reaction Steps

8 ml of hydrochloric ethyl ether (1 M) are added to the solution of 1.92 g (4.05 mmol) of the imine obtained in stage A above in a mixture of 40 ml of dichloromethane and 8 ml of methanol. The clear orange medium becomes dark red and then a precipitate forms. After 1 hour at ambient temperature, the precipitate is filtered and then washed with dichloromethane and dried under vacuum at 50° C., to give 1.18 g (84%) of the hydrochloride in the form of an ochre powder.

Provenance & Evidence