HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxyethylamine → HCID 67506721, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxyethylamine | HCID 8018 | — |
| Reactant | 4-Fluoro-3-nitro-1,1'-biphenyl | HCID 10680271 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 67506721 | HCID 67506721 | — |
Reaction Steps
2-methoxyethaneamine (1.5 mL) is added to a solution of 4-fluoro-3-nitrobiphenyl (200 mg, 0.92 mmol) in ethanol. The reaction may be stirred at room temperature overnight and concentrated. The residue may be purified by any appropriate method, such as Biotage column chromatography to give N-(2-methoxyethyl)-3-nitrobiphenyl-4-amine (228 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09125901B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-e8320db504304256876ba8993e0abf19 |
| Source note | uspto-grants-2015_09 |